plc controlled experimental supercritical fluid_extraction equipment

HA220-50-10C Supercritical co2 extraction equipment

Supercritical co2 extraction machine, system,for Aloe Vera & Essential oil

Pilot scale supercritical co2 extraction systems

Extraction kettle:Material: 0Cr18Ni9;

Volume: 5L 2 set;

Maximum working pressure: 50MPa.

Separation tank:Material: 0Cr18Ni9;

Volume: 2L,2L 2sets;

Maximum working pressure: 30MPa.

Description:

HA220-50-10C is very popular in small factories.

It has 2 extraction kettles with a capacity of 5L, and the designed maximum pressure is 50MPa. The two extraction kettles work alternately. After each extraction, the excess CO2 in the extraction kettle can be transferred to another kettle, thereby saving CO2.

The high-pressure valve adopts the Emerson 1700 series and the reliable and stable high-pressure pump

Supercritical co2 extraction equipment
HA120-50-10C Supercritical co2 extraction equipment

Supercritical fluid is a kind of non-gaseous and non-liquid state between gas and liquid, which can only exist when its temperature and pressure exceed the critical point. Supercritical fluids are dense, similar to liquids, and their viscosities are close to gases. Therefore, supercritical fluid is an ideal extractant.

Huaan can flexibly configure one: 1L+10L (10L -100L)supercritical fluid extraction pilot system ( Equipment pictures ) , which enables feasibility study, process development, parameter amplification, and pilot production to be completed in the same unit without additional investment.

Supercritical co2 extraction equipment
HA120-50-10C Supercritical co2 extraction equipment

Different applications and different companies have very different requirements for the pilot level. The pilot is a step in the design of production equipment. Therefore, Huaan Supercritical emphasizes flexibility and flexibility when designing and developing pilot systems. Cost efficiency. The flexible design of Huaan's supercritical system makes the optimization of test and process parameters more convenient.

Supercritical co2 extraction equipment
HA120-50-10C Supercritical co2 extraction equipment

Huaan has customized thousands of pilot plants for many university laboratories and enterprises around the world.

supercritical co2 extraction machine includes several parts:

Main configuration

No.

Name

Specification

1

Extraction kettle

1.Volume:10L;

2.Temperature: room temperature to 80 C, automatic control of heating temperature, measurement of CO2 fluid temperature;

3. Material: 0Cr18Ni9.

2

Separation kettle

Equipped with water jacketed circulating heating system, temperature adjustable

Material 0Cr18Ni9

Specifications:2l,2L 30Mpa

3

CO2 high pressure pump (frequency modulation)

Flow specification (double plunger) 0—50L/h adjustable frequency conversion

Maximum working pressure40Mpa pump head with cooling system

Quantity 1 set

4

Entrainer pump

Flow specification (double plunger) 1/4-4L/h mechanical adjustment

Maximum working pressure40MPa

5

Refrigeration system

Cooling capacity 3300Kcal/h air cooling

Temperature control range -5°C~+5°C to meet process requirements

6

Heat exchange system

Material 0Cr18Ni9

Maximum working pressure40MPa

7

Purification system

Material 0Cr18Ni9

Maximum working pressure40MPa

8

CO2 storage tank

Material 0Cr18Ni9

Specifications 4L/16MPa

9

Flow meter

Specifications Metal tube float flowmeter 10-100L/h

Digital remote transmission shows instantaneous flow and cumulative flow respectively

10

Temperature Control System

Control range Adjustable from room temperature to 75 °C (water bath)

Temperature control accuracy ±1 °C digital display dual screen

11

Safety protection device

1. High-pressure pump outlet distribution contact pressure gauge, set working pressure, over-pressure automatic stop pump protection.

2. The high pressure pump, the extraction kettle, the separation kettle and the rectification column are respectively equipped with safety valves and overpressure automatic pressure relief protection according to the highest working pressure.

12

Atmospheric pressure Electric heating hot water boiler

12. Pipeline:

The container, valve, pipe fittings and pipelines that contact the fluid are made of 0Cr18Ni9 stainless steel. The valve stem of the valve is specially heat-treated and durable.

13

Instrument features

1. The extraction kettle pressure ring opens quickly.

2. CO2 is recycled.

14

Other

1. Power supply: three-phase four-wire system 380V/50HZ total power 18Kw

2. CO2: food grade ≥99.5%, single bottle net weight ≥22Kg

3. Installation size: 3000 × 2000 × 1700m / m, plus operating space.

Process Design:

Supercritical co2 extraction machine
HA120-50-10C Supercritical co2 extraction equipment

Liquid Co2 from pressured bottle or storage tank, through pipeline into purifying part, cooling part, mixer part, after heated and transferred into extractor, where solid raw material loading into barrel feeding into extractor, with dissolve ability to extracting, through temperature and pressure condition change, separated target material in separator. Separated material without chemical solution remained, Co2 would be gasifying after few seconds.

Supercritical co2 extraction machine
HA120-50-10C Supercritical co2 extraction equipment

Application:

Supercritical Co2 Fluid Extraction mianly applied in many different material extraction:

1. flower essential oil: Lavander, rose

2. fruit frangrance: pectin, phenols

3. spice : garlic or pepper oil

4. natural leaves: tea polyphenols, olive leaf oil

5. natural pigment: capsorubin, curcumin

6. plant seeds: The wheat shoots blanks oil, Sea-buckthorn oil

7. high value product: propolis, astaxanthin

CO2 high pressure pump:

CO2 high pressure pump for Supercritical co2 extraction equipment
CO2 high pressure pump

Huaan high-pressure carbon dioxide injection pumps are low-speed reciprocating high-pressure pumps, using zirconia three-plunger structure, as the key equipment of Supercritical CO2 CBD extraction system, can be widely used in biological, pharmaceutical, food and other fields.

Has the characteristics of stable pressure, small volume, high efficiency, beautiful appearance, convenient operation and maintenance, portable and flexible.

Cooling system:

Cooling system for Supercritical co2 extraction equipment
Cooling system

Cooling system integrates compressor, heat exchanger, cooler and circulating system. It has compact design, reduces occupied space, reduces energy loss, improves cooling efficiency and ensures stable liquid carbon dioxide supply. Environmental friendly refrigerant R407C is used.

High precision pressure regulator:

High precision pressure regulator for Supercritical co2 extraction equipment
High precision pressure regulator

Pressure Manual Controller: The back pressure valve of TESCOM 26-1700 series is adopted. The valve has high pressure control precision and long service life.

Supercritical co2 extraction equipment

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