plc controlled experimental supercritical fluid_extraction equipment

HA330-40-72 Supercritical co2 extraction equipment

Supercritical co2 extraction machine, system, for CBD oil

Pilot scale supercritical co2 extraction systems

Extraction kettle:Material: 0Cr18Ni9;

Volume: 24L 3 set;

Maximum working pressure:40MPa.

Separation kettle:Material: 0Cr18Ni9;

Volume: 10L 3sets;

Maximum working pressure: 30MPa.

CO2 extraction machine

Description:

Huaan can flexibly configure one: 1L+10L (10L -100L)supercritical fluid extraction pilot system , which enables feasibility study, process development, parameter amplification, and pilot production to be completed in the same unit without additional investment.

Different applications and different companies have very different requirements for the pilot level. The pilot is a step in the design of production equipment. Therefore, Huaan Supercritical emphasizes flexibility and flexibility when designing and developing pilot systems. Cost efficiency. The flexible design of Huaan's supercritical system makes the optimization of test and process parameters more convenient.

Huaan has customized thousands of pilot plants for many university laboratories and enterprises around the world.

HA330-40-72 Supercritical co2 extraction equipment is a supercritical fluid extraction pilot system produced by Huaan, which enables feasibility study, process development, parameter amplification and pilot production to be completed in the same unit without additional investment.Simple and intuitive software, friendly interface.High self-control level, stable and reliable product quality and experimental data, suitable for industrial scale design basis and small-scale production.

HA330-40-72 Supercritical co2 extraction equipment is composed of CO2 supply system, extraction and separation system, CO2 circulation system, clean system, co-solvent system, cold water circulation system, hot water circulation system, steel platform, control system, tail gas recovery system, and so on.

Supercritical co2 extraction equipment
HA330-40-72 Supercritical co2 extraction equipment

CO2 supply system

Put liquid CO2 by delivery pump to condenser before or during operation. The CO2 supply system contains: outside CO2 delivery pump, outside tank.

Extraction and separation

The liquid CO2 flow through pre-heater to heat after pump by CO2 high pressure pump, then flow to extractor, the outlet temperature will be controlled automatic.

CO2 circulation system

The CO2 will back to middle storage tank after finish extraction, waiting the pressure balance between extractor and middle tank at 50bar, then put the left CO2 of extractor to the next extractor

Clean system working

Pump the clean agent to pipes from clean tank when finish extraction working.The clean system is composed of clean storage tank, clean pump.

Cold water circulation system

Pump tap water to purified water equipment, it flows to cold water tank after purifying. Pump cold purified water to refrigerator, the water will back to cold water tank after cooling.Hot water circulation system

Put soften water to hot water tank, start hot water circulation pump and heated by electro-boiler(or heated by vapor), then distribute the hot water to extractor, separator, heat exchanger by the use of hot water circulation pump.

Steel platform description

The steel platform is for device fix and operation.With carbon steel, and antirust paint, the plane and stair is stainless steel riffled plate.

Tail gas recovery system

When extraction finish, close CO2 high pressure pump, the CO2 of extractor and separator will flow back to middle tank, when pressure balance, let the CO2 of extractor to another extractor, and pump the residual CO2 by compressor when pressure balance between two extractors.

Control system description

The control system is composed of low voltage switch box, PLC control cabinet, extractor quick-open chain control cabinet, control computer, cooling unit control cabinet, and so on.

Supercritical fluid extraction equipment
HA330-40-72 Supercritical fluid extraction equipment

Main configuration

No.

Name

Specification

1

Extraction kettle

Material: 0Cr18Ni9.

Volume:24L,3sets;

Maximum working pressure:40MPa.

2

Separation kettle

Equipped with water jacketed circulating heating system, temperature adjustable;

Material: 0Cr18Ni9;

Volume:10L, 3sets;

Maximum working pressure: 30MPa.

3

CO2 high pressure pump

Flow specification (three plunger) : 0—400L/h, adjustable frequency conversion

Maximum working pressure:40Mpa, pump head with cooling system.

4

Entrainer pump

Flow specification (double plunger): 1/4-20L/h, mechanical adjustment;

Maximum working pressure: 40MPa

5

Refrigeration system

Cooling capacity: 15000Kcal/h, air cooling or water cooling;

Temperature control range: -5°C~+5°C to meet process requirements.

6

Heat exchange system

Material: 0Cr18Ni9;

Specification: Φ14、Φ18;

Maximum working pressure:40MPa、30MPa.

Equipped with water jacketed circulating heating system, temperature adjustable.

7

CO2 storage tank

Material: 0Cr18Ni9;

Volume:20L, 1 set;

Maximum working pressure: 16MPa.

8

Level gauge

Material: 0Cr18Ni9;

Maximum working pressure: 16MPa.

9

Flow meter, accumulator

Specifications: metal tube float flowmeter, digital remote transmission.

Digital display: display instantaneous and cumulative flow respectively.

10

Temperature Control System

Control range: adjustable from room temperature to 75 °C (water bath).

Dynamic temperature control accuracy: ±1 °C, digital display dual screen.

11

Safety protection device

1. High-pressure pump outlet distribution contact pressure gauge, set working pressure, over-pressure automatic stop pump protection.

2. The extraction kettle, the separation kettle and the storage tank are respectively equipped with safety valves and overpressure automatic pressure relief protection according to the highest working pressure.

12

Purification system

Material: 0Cr18Ni9;

Maximum working pressure: 5L/16MPa.

13

Barrel lifting system

Equipped with electric hoist for loading and unloading of material cylinders.

14

Pipeline

Valves、fittings: DW14 and DW18 respectively.

The container, valve, pipe fittings and pipelines that contact the fluid are made of 0Cr18Ni9 stainless steel. The valve stem of the valve is specially heat-treated and durable.

15

Instrument features

1. The extraction kettle pressure ring opens quickly.

2. CO2 is recycled.

16

Power supply、air source

1. Power supply: three-phase four-wire system 380V/50HZ (can be customized other power supply), total power BR230-50-48 is 35KW, normal operation is 16KW.

2. CO2: food grade ≥ 99.5%, single bottle net weight ≥ 22Kg, User-supplied.

17

Installation size

The device is modular installation, installation size (length × width × height): 5.5 × 5 × 4m, plus operating space.

Advantages:

Supercritical co2 extraction machine
HA330-40-72 Supercritical co2 extraction machine

Convenient in operation. Can be used widely.

With an excellent optional function. Extracts can be gained optionally by controlling the pressure and temperature.

Low operation temperature. Can be extracted near to the room temperature, especially fit for the extracting of thermo-sensitive elements. The possibility of oxidation when contact with oxygen and reaction when meet rays are eliminated. The natural flavor of the extracts can be kept.

Extracting media and extracts can be separated easily. No leftover of CO2 on the extracts after extracting operation.

CO2 is a nontoxic, flavorless, noncombustible and cheap compound and can be recycle used.

Application:

Range of Application
Type of Application
Pharmaceutical Industry
Extraction of effective contents of Chinese herbs, concentration, refinement and precipitation of raw material drug, separation and refinement of fatty mixtures.
Foodstuff Industry
Extraction of hops, caffeine removal from coffee berry, extraction of plant
Cosmetics and Perfumery Industry
Separation and refinement of natural and synthetic perfumeries, dealkalization of tobacco, extraction of raw material cosmetics.
Chemical Industry
Separation of hydrocarbon, refinement of organic synthetic raw material, separation of azeotrope, retrieval of raw materials of reaction, dehydration of water soluble powder of organic solution, water oxidation.
Others
Superconducting, semiconductor, ceramics, oil washing of petroleum core, enzyme catalytic reaction, preparation of materials, superfine granules, extraction of complex compound, supercritical dyeing technique, supercritical reaction, supercritical coating technique (pharmacy-making). 

Extraction seasources :

Seabuckthorn fruit oil,wheat embryo oil,medlar seed oil, grape seed oil,oidiophore oil of glossy ganoderma,kiwifruit oil,seed oil of job’s tears,walnut oil.seed oil of forest frog,fish oil,pine pollen oil,cauliflower oil

Arteannuin,sundrops oil,angelica sinensis oil,chuanxiong rhizome oil,clove oil,atractylis oil,zedoary turmeric oil,dahurian angelica oil,cinnamon leafoil,zedoary turmeric oil,dahurian angelica oil,cinnammonleaf oil,ginkgo oil.netmeg oil,menthence,schisandra oil,plantain seed oil,radix buple chrysanthemum oil,Salvia miltiorrhiza extract,herba Andrographis extract,curcuma oil pigment,lycopin,bee glue,antibiotics precipitation,Rhizoma Alismatis oil,yolk powder phospholipid,cortex magnoliae.officinalis extract,olibanum extract,natural caffeine,Srcandra hainanensis extract,cyperus oil,maloicacid,houttuynia cordata oil

Gingerol,pepper haematochrome,dried tiny shrimp haematochrome,zanthoxylum oil,allspice oil resin,onion root oil,garlic oil,hops extract,tobacco leaves essencial oil

Supercritical co2 extraction equipment

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